An Overview on Steps of Pesticide Residue Analysis and Contribution of the Individual Steps to the Measurement Uncertainty

dc.authorid Omeroglu, Perihan Yolci/0000-0001-8254-3401
dc.authorid BOYACIOGLU, DILEK/0000-0002-8160-0619
dc.authorscopusid 55207260400
dc.authorscopusid 6507544176
dc.authorscopusid 7003689519
dc.authorscopusid 6602229012
dc.authorscopusid 25947697200
dc.authorwosid Omeroglu, Perihan Yolci/AAG-8517-2021
dc.authorwosid BOYACIOGLU, DILEK/G-5552-2012
dc.authorwosid Boyacioglu, Dilek/AAX-8482-2020
dc.contributor.author Omeroglu, Perihan Yolci
dc.contributor.author Boyacioglu, Dilek
dc.contributor.author Ambrus, Arpad
dc.contributor.author Karaali, Artemis
dc.contributor.author Saner, Samim
dc.date.accessioned 2024-05-25T11:24:12Z
dc.date.available 2024-05-25T11:24:12Z
dc.date.issued 2012
dc.department Okan University en_US
dc.department-temp [Omeroglu, Perihan Yolci] Okan Univ, Dept Food Engn, Fac Engn & Architecture, TR-34959 Istanbul, Turkey; [Boyacioglu, Dilek] Istanbul Tech Univ, Dept Food Engn, Fac Chem & Met Engn, TR-34469 Istanbul, Turkey; [Ambrus, Arpad] Hungarian Food Safety Off, H-1097 Budapest, Hungary; [Karaali, Artemis] Yeditepe Univ, Dept Food Engn, Fac Engn & Architecture, TR-34755 Istanbul, Turkey; [Saner, Samim] Kalite Sistem Labs Grp, TR-34742 Istanbul, Turkey en_US
dc.description Omeroglu, Perihan Yolci/0000-0001-8254-3401; BOYACIOGLU, DILEK/0000-0002-8160-0619 en_US
dc.description.abstract To facilitate the international food trade as well as to protect consumers from exposure to unacceptable pesticide residue levels, Codex Alimentarius Commission, European Union, and National Authorities set maximum residue limits for different food commodities. The control of pesticide residues at national and international level requires reliable and comparable analytical data that can be obtained by applying validated methods and implementing an effective internal quality control and quality assurance system in the testing laboratories. For the correct interpretation of the analytical results, measurement uncertainty should be estimated. Pesticide residue analysis includes two main steps: sampling performed outside of the laboratory and laboratory operations comprising of sample preparation, sample size reduction, sample processing, extraction, cleanup, and chromatographic determination. By taking into consideration the contribution of the individual steps to the overall uncertainty of the results, the analytical procedures can be optimized to fit for the purpose of the analysis with minimum cost. The scope of this paper is to review major steps of pesticide residue analysis in the light of current developments, to highlight the importance of identification and estimation of the uncertainties associated with the results, to describe suitable methods for their estimation, and to summarize the contribution of each step to the combined uncertainty. en_US
dc.identifier.citationcount 20
dc.identifier.doi 10.1007/s12161-012-9396-4
dc.identifier.endpage 1480 en_US
dc.identifier.issn 1936-9751
dc.identifier.issn 1936-976X
dc.identifier.issue 6 en_US
dc.identifier.scopus 2-s2.0-84867669466
dc.identifier.scopusquality Q2
dc.identifier.startpage 1469 en_US
dc.identifier.uri https://doi.org/10.1007/s12161-012-9396-4
dc.identifier.uri https://hdl.handle.net/20.500.14517/786
dc.identifier.volume 5 en_US
dc.identifier.wos WOS:000310028600030
dc.identifier.wosquality Q3
dc.language.iso en
dc.publisher Springer en_US
dc.relation.publicationcategory Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı en_US
dc.rights info:eu-repo/semantics/closedAccess en_US
dc.scopus.citedbyCount 20
dc.subject Pesticide en_US
dc.subject Pesticide residue analysis en_US
dc.subject Uncertainty en_US
dc.title An Overview on Steps of Pesticide Residue Analysis and Contribution of the Individual Steps to the Measurement Uncertainty en_US
dc.type Article en_US
dc.wos.citedbyCount 19

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